MS Report from Instrument: LCMS-03 File ..3\\Data\\20170920\\20170920\\BIZ2017-920-WYQ7.D Tgt Mass (CHM): Injection Date : 20 Sep 17 12:10 pm +0800 Seq. Line : 40 Sample Name : BIZ2017-920-WYQ7 Location : P1-C-04 Acq. Operator : SYSTEM Inj : 1 Spec. Reported : MS Integration Inj Volume : 1.5 ul Acq. Method : D:\\LCMS03\\Data\\20170920\\20170920\\1-POS-3MIN.M Analysis Method : D:\\LCMS03\\Data\\20170920\\20170920\\1-POS-3MIN.M Catalog No : HY-14167 Batch#26380 Method Info : Mobile Phase: A: water(0.01%TFA) B:ACN(0.01%TFA) Gradient: 5% to 95%B within 1.3 min Flow Rate :1.8ml/min Column :SunFire C18, 4.6*50mm,3.5um A-RP-186 Oven Temperature : 45C DAD1 A, Sig=214,4 Ref=off1.9161.993mAU200000.5 DAD1 B, Sig=254,4 Ref=offmAU1.422100000.5 ELS1 A, ELSD SignalmV1005000.51 MSD1 TIC, MS File ES-API, Pos, Scan, Frag: 701.51.94522.5min111.51.91622.5min1.9921.51.98122.5min2000000000.51 Ion 448, MSD1 448,Target Mass 448 Positive, EIC=447.7:448.715001000500000.511.522.5min Integration Results for DAD1 A, Sig=214,4 Ref=off1.522.5min RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.92 0.02 415.40 388.38 99.97 449 1.99 0.01 0.11 0.06 0.03 449 Integration Results for DAD1 B, Sig=254,4 Ref=off RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.42 0.01 0.49 0.62 0.18 582 1.92 0.02 271.19 252.69 99.79 449 1.99 0.01 0.07 0.10 0.03 449 Integration Results for MSD1 TIC, MS File RetTim Width Area Height Area% MS(+)|-------|--------|--------------|--------------|--------|------| 1.94 0.06 12802579.00 3483259.75 100.00 449LCMS-03 9/21/2017 9:04:05 SYSTEMPage1 of3MS Report from Instrument: LCMS-03Ret. Time: 1.94 <<<< POSITIVE SPECTRA >>>> ES-API Positive449.1451.1105.1179.2233.1305.1450.1472.1471.1514.1338.4400000350000300000250000200000150000100000500000100200300400500600700800900m/zLCMS-03 9/21/2017 9:04:05 SYSTEMPage2 of3MS Report from Instrument: LCMS-03 *** End of Report ***LCMS-03 9/21/2017 9:04:05 SYSTEMPage3 of3